Roflumilast-N-oxide-LCMS-27623-MedChemExpress.pdf

1、 File .Data2017120520171205-2BIZ2017-D05-WYQ5.D Tgt Mass (CHM):Injection Date : 5 Dec 17 5:47 pm +0800 Seq. Line : 38Sample Name : BIZ2017-D05-WYQ5 Location : P2-A-07Acq. Operator : ZLJ_587 Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:LCMS03Data2017120520171205-21-POS-3MIN

2、.MAnalysis Method : D:LCMS03Data2017120520171205-21-POS-3MIN.MCatalog No : HY-100639 Batch#27623Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temperature : 45Cmin0 0.5 1 1.5 2 2.5m

3、AU05001000DAD1 A, Sig=214,4 Ref=off1.6411.7071.897min0 0.5 1 1.5 2 2.5mAU0100200DAD1 B, Sig=254,4 Ref=off1.7071.897min0 0.5 1 1.5 2 2.5mV0100ELS1 A, ELSD Signal1.777min0 0.5 1 1.5 2 2.5010000002000000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.741min0 0.5 1 1.5 2 2.50250000500000750000Ion 419, MS

4、D1 419,Target Mass 418 +H Positive, EIC=418.7:419.71.739Integration Results for DAD1 A, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.64 0.02 0.92 0.87 0.04 2331.71 0.02 2084.50 1628.09 99.69 4191.90 0.02 5.60 4.95 0.27 233Integration Results for DAD1 B, Sig=254,4 Ref=offRetTim

5、 Width Area Height Area% MS(+)|-|-|-|-|-|-|1.71 0.02 374.94 290.92 99.65 4191.90 0.02 1.30 1.34 0.35 233Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.74 0.06 10667483.00 2684906.25 100.00 419MS Report from Instrument: LCMS-03LCMS-03 12/6/2017 9:14:43 ZLJ

6、_587 Page 1 of 3Ret. Time: 1.74 m/z100 200 300 400 500 600 700 800 900050000100000150000200000250000ES-API Positive859.0579.0443.0423.1421.0419.1MS Report from Instrument: LCMS-03LCMS-03 12/6/2017 9:14:43 ZLJ_587 Page 2 of 3* End of Report *MS Report from Instrument: LCMS-03LCMS-03 12/6/2017 9:14:43 ZLJ_587 Page 3 of 3