Fingolimod-hydrochloride-LCMS-26663-MedChemExpress.pdf

1、 File .3Data2017101720171017BIZ2017-O16-WYQ2.D Tgt Mass (CHM):Injection Date : 17 Oct 17 10:12 am +0800 Seq. Line : 18Sample Name : BIZ2017-O16-WYQ2 Location : P1-A-10Acq. Operator : SYSTEM Inj : 1Spec. Reported : MS Integration Inj Volume : 2 ulAcq. Method : D:LCMS03Data20171017201710171-POS-3MIN.M

2、Analysis Method : D:LCMS03Data20171017201710171-POS-3MIN.MCatalog No : HY-12005 Batch#26663Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temperature : 45Cmin0 0.5 1 1.5 2 2.5mAU020

3、0DAD1 A, Sig=214,4 Ref=off0.5341.599min0 0.5 1 1.5 2 2.5mAU05DAD1 B, Sig=254,4 Ref=offmin0 0.5 1 1.5 2 2.5mV0200ELS1 A, ELSD Signal1.670min0 0.5 1 1.5 2 2.50200000040000006000000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.636min0 0.5 1 1.5 2 2.505001000Ion 343.2, MSD1 343.2,Target Mass 343.2 Posi

4、tive, EIC=342.9:343.9Integration Results for DAD1 A, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|0.53 0.01 2.76 3.95 0.24 4491.60 0.04 1131.84 443.35 99.76 308Integration Results for DAD1 B, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|Integration Results f

5、or MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.64 0.08 31980280.00 6349144.00 100.00 308MS Report from Instrument: LCMS-03LCMS-03 10/17/2017 11:03:40 SYSTEM Page 1 of 3Ret. Time: 1.64 m/z100 200 300 400 500 600 700 800 90002000004000006000008000001E61.2E61.4E61.6E6ES-API Positive312.1309.1308.1MS Report from Instrument: LCMS-03LCMS-03 10/17/2017 11:03:40 SYSTEM Page 2 of 3* End of Report *MS Report from Instrument: LCMS-03LCMS-03 10/17/2017 11:03:40 SYSTEM Page 3 of 3