GBR-12935-dihydrochloride-LCMS-12547-MedChemExpress.pdf

1、 File .710 2017-07-10 08-26-50CPK2017-707-12547.D Tgt Mass (CHM): Injection Date : 10 Jul 17 7:38 pm +0800 Seq. Line : 148Sample Name : CPK2017-707-12547 Location : P1-F-08Acq. Operator : ZLJ_587 Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:chem321DATA2017071020170710 2017

2、-07-10 08-26-501-POS-3MIN.MAnalysis Method : D:CHEM321DATA2017071020170710 2017-07-10 08-26-501-POS-3MIN.MCatalog No : HY-12242 Batch#12547 A-RP-186Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um

3、 A-RP-186Oven Temperature : 45Cmin0.5 1 1.5 2 2.5mAU0200400DAD1 B, Sig=214,4 Ref=off 0.427 0.693 1.4561.4861.656min0.5 1 1.5 2 2.5mAU010DAD1 C, Sig=254,4 Ref=off 1.3051.4872.077min0.5 1 1.5 2 2.50100000200000300000400000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.515min0.5 1 1.5 2 2.50100200Ion 4

4、88.5, MSD1 488.5,Target Mass 487.5 +H Positive, EIC=488.2:489.2 Integration Results for DAD1 B, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|0.43 0.02 1.83 0.31 0.15 ND0.69 0.03 4.70 -0.20 0.37 ND1.46 0.01 0.47 0.81 0.04 ND1.49 0.03 1242.55 674.30 98.90 4151.66 0.03 6.82 3.76 0.

5、54 415Integration Results for DAD1 C, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.30 0.03 2.43 1.18 5.47 ND1.49 0.03 41.83 21.45 94.00 4152.08 0.01 0.24 0.29 0.53 415Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.51 0.05 1154280.38

6、 424707.41 100.00 415MS Report from Instrument: LCMS-02LCMS-02 7/14/2017 10:59:18 ZLJ_587 Page 1 of 2Ret. Time: 1.51 m/z200 300 400 500 600 700 800 9000100002000030000400005000060000700008000090000ES-API Positive167.1249.2416.3415.3MS Report from Instrument: LCMS-02LCMS-02 7/14/2017 10:59:18 ZLJ_587 Page 2 of 2