1、 File D:CHEM321DATA20170306HECGCY4076-009-5.D Tgt Mass (EZX): Injection Date : 6 Mar 17 1:11 pm +0800 Seq. Line : 0Sample Name : GCY4076-009-5 Location : P2-B-05Acq. Operator : GZZ_718 Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:Chem321METHODS1-POS-3MIN.MAnalysis Method :
2、 D:CHEM321METHODS1-POS-3MIN-PROSRSS.MCatalog No : HY-13578 Batch#23884 Easy-Access Method: 1-POS-3MINMethod Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temperature : 45Cmin*0.5 1 1.5 2
3、2.5mAU0100200300400*DAD1 B, Sig=214,4 Ref=off 1.2951.3491.4881.6541.801min*0.5 1 1.5 2 2.5mAU02004006008001000*DAD1 C, Sig=254,4 Ref=off 1.3031.3491.507 1.635 1.802min0.5 1 1.5 2 2.5050001000015000200002500030000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.332Integration Results for DAD1 B, Sig=21
4、4,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.30 0.01 0.83 0.01 0.12 ND1.35 0.02 699.10 550.61 98.72 3551.49 0.02 6.85 -0.02 0.97 ND1.65 0.02 0.78 0.09 0.11 ND1.80 0.02 0.59 0.14 0.08 NDIntegration Results for DAD1 C, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|
5、1.30 0.02 3.16 2.14 0.19 ND1.35 0.02 1679.21 1299.35 99.55 3551.51 0.03 0.73 0.41 0.04 ND1.64 0.04 1.52 0.15 0.09 ND1.80 0.02 2.24 0.05 0.13 NDMS Report from Instrument: HY-LCMS-02HY-LCMS-02 3/10/2017 2:37:15 PM GZZ_718 Page 1 of 2Ret. Time: 1.33 m/z200 300 400 500 600 700 800 9000500100015002000ES-API Positive116.2233.3340.5709.0814.5366.2 492.9216.9117.2356.9MS Report from Instrument: HY-LCMS-02HY-LCMS-02 3/10/2017 2:37:15 PM GZZ_718 Page 2 of 2
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