AC-55541-LCMS-13693-MedChemExpress.pdf

1、 File .7-2 2017-07-07 15-32-44CPK2017-707-13693.D Tgt Mass (CHM): Injection Date : 7 Jul 17 6:16 pm +0800 Seq. Line : 37Sample Name : CPK2017-707-13693 Location : P1-E-06Acq. Operator : ZLJ_587 Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:chem321DATA2017070720170707-2 2017

2、-07-07 15-32-441-POS-3MIN.MAnalysis Method : D:CHEM321DATA2017070720170707-2 2017-07-07 15-32-441-POS-3MIN.MCatalog No : HY-14350 Batch#13693 A-RP-186Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5

3、um A-RP-186Oven Temperature : 45Cmin0.5 1 1.5 2 2.5mAU050010001500DAD1 B, Sig=214,4 Ref=off 1.288 1.658 1.7301.781min0.5 1 1.5 2 2.5mAU0200400600DAD1 C, Sig=254,4 Ref=off 1.665 1.7311.781min0.5 1 1.5 2 2.5050000100000150000200000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.773min0.5 1 1.5 2 2.5010

4、0002000030000Ion 519.4, MSD1 519.4,Target Mass 518.4 +H Positive, EIC=519.1:520.1 1.802 1.817Integration Results for DAD1 B, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.29 0.02 6.84 0.19 0.23 1571.66 0.02 6.58 0.06 0.22 ND1.73 0.02 5.83 4.02 0.20 ND1.78 0.03 2925.22 1861.15 9

5、9.35 518Integration Results for DAD1 C, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.67 0.02 2.96 0.10 0.23 ND1.73 0.02 2.39 1.65 0.18 ND1.78 0.03 1304.90 838.71 99.59 518Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.77 0.04 183651.64 1433.15 100.00 518MS Report from Instrument: LCMS-02LCMS-02 7/13/2017 18:13:16 ZLJ_587 Page 1 of 2Ret. Time: 1.77 m/z200 300 400 500 600 700 800 900020004000600080001000012000ES-API Positive521.0520.0MS Report from Instrument: LCMS-02LCMS-02 7/13/2017 18:13:16 ZLJ_587 Page 2 of 2