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1、(怀椁匀%椁椁怀椁讀缁缀幨砀螏頀h椀餂謃圊權猊猊猊鬊鬊鬊鬊鬊鬊鬊鬊鬊鬊鬊鬊鬊鬊鬊鬊鬊鬊鴊娀一刀攀搀栀攀洀砀瀀爀攀猀猀瀀搀昀瀀椀挀最椀昀娀一刀攀搀栀攀洀砀瀀爀攀猀猀瀀搀昀尀尀挀搀搀愀挀攀搀搀愀戀挀挀戀戀洀戀唀唀洀倀洀昀渀吀琀樀礀昀椀搀圀倀渀堀眀儀伀一戀氀氀礀吀嘀氀栀娀儀娀一刀攀搀栀攀洀砀瀀爀攀猀猀昀攀戀昀昀搀戀戀挀搀瀀瀀洀琀愀琀攀瀀爀漀挀甀洀攀渀琀猀吀椀琀氀攀愀琀愀氀漀最一漀夀愀琀挀栀匀瀀攀挀琀爀甀洀吀椀琀氀攀倀爀攀焀甀攀渀挀礀稀昀伀爀椀最椀渀愀氀倀漀椀渀琀猀漀甀渀琀昀挀琀甀愀氀倀漀椀渀琀猀漀甀渀琀昀挀焀甀椀猀椀琀椀漀渀吀椀洀攀猀攀挀昀匀瀀攀挀琀爀愀氀圀椀搀琀栀瀀瀀洀昀倀甀氀猀攀倀爀漀最爀愀洀唀

2、渀欀渀漀眀渀匀愀洀瀀氀攀倀愀琀愀氀漀最一漀夀愀琀挀栀匀伀伀伀一刀刀一攀搀栀攀洀砀瀀爀攀猀猀靓言茀渀7椁:胔-检輀%棙i缀$AZD9496-HNMR-17191-MedChemExpress.pdfpic1.gifAZD9496HNMR17191MedChemExpress.pdf2019-61129cd07da-ce0d-43d5-a42b-cc385432bb66m9LbKAUUEmPmFfnTt9jyf2idWJ8C1PInHXwQON/blA7lJyTHVlhZ9Q=AZD9496,HNMR,17191,MedChemExpress010feb62976f43fd5327213b8bc2

3、43d9ppm (t1)0.01.02.03.04.05.06.07.08.09.010.011.012.012.62012.614 12.608 12.602 12.596 12.594 12.587 12.583 12.578 12.575 12.569 12.559 12.539 10.581 7.557 7.517 7.469 7.443 7.418 7.399 7.189 7.170 6.999 6.982 6.979 6.965 6.947 6.685 6.645 3.514 3.500 3.342 2.918 2.881 2.599 2.588 2.561 2.550 2.504

4、 2.500 2.496 2.392 2.354 2.332 2.296 1.227 1.173 1.148 1.095 1.055 1.0391.0001.062 1.995 1.042 1.021 2.054 1.010 1.167 2.076 1.129 1.193 3.054 3.135 3.2930.9740.807Date:16 Apr 2018Documents Title:Catalog No : HY-12870 Batch#17191Spectrum Title:CPK2018-413-17191Frequency (MHz):(f1) 400.130 Original P

5、oints Count:(f1) 32768 Actual Points Count:(f1) 32768 Acquisition Time (sec):(f1) 3.2768 Spectral Width (ppm):(f1) 24.992 Pulse Program:UnknownSample ID:CPK2018-413-17191, Catalog No : HY-12870 Batch#17191, DMSOOOHHN(R)(R)NFFF(E)HHMedChemExpress0001500006-20190611085439704331A%椁椁怀椁讀缁缀幨砀螏頀h栀$AZD9496-

6、HNMR-17191-MedChemExpress.pdfpic1.gifAZD9496HNMR17191MedChemExpress.pdf2019-61129cd07da-ce0d-43d5-a42b-cc385432bb66m9LbKAUUEmPmFfnTt9jyf2idWJ8C1PInHXwQON/blA7lJyTHVlhZ9Q=AZD9496,HNMR,17191,MedChemExpress010feb62976f43fd5327213b8bc243d9ppm (t1)0.01.02.03.04.05.06.07.08.09.010.011.012.012.62012.614 12

7、.608 12.602 12.596 12.594 12.587 12.583 12.578 12.575 12.569 12.559 12.539 10.581 7.557 7.517 7.469 7.443 7.418 7.399 7.189 7.170 6.999 6.982 6.979 6.965 6.947 6.685 6.645 3.514 3.500 3.342 2.918 2.881 2.599 2.588 2.561 2.550 2.504 2.500 2.496 2.392 2.354 2.332 2.296 1.227 1.173 1.148 1.095 1.055 1.

8、0391.0001.062 1.995 1.042 1.021 2.054 1.010 1.167 2.076 1.129 1.193 3.054 3.135 3.2930.9740.807Date:16 Apr 2018Documents Title:Catalog No : HY-12870 Batch#17191Spectrum Title:CPK2018-413-17191Frequency (MHz):(f1) 400.130 Original Points Count:(f1) 32768 Actual Points Count:(f1) 32768 Acquisition Tim

9、e (sec):(f1) 3.2768 Spectral Width (ppm):(f1) 24.992 Pulse Program:UnknownSample ID:CPK2018-413-17191, Catalog No : HY-12870 Batch#17191, DMSOOOHHN(R)(R)NFFF(E)HHMedChemExpress0001500006先进医疗20190611085439704331A(怀椁匀%椁椁怀椁讀缁缀幩砀螏頀h怀椀餂謃笃笝笝霝娀匀攀搀栀攀洀砀瀀爀攀猀猀瀀搀昀瀀椀挀最椀昀娀匀攀搀栀攀洀砀瀀爀攀猀猀瀀搀昀尀尀挀攀愀挀戀昀戀昀搀砀眀栀唀洀猀吀刀椀刀樀甀儀愀匀

10、琀攀刀倀樀欀愀堀洀瀀吀嘀挀一搀漀戀倀礀娀儀娀匀攀搀栀攀洀砀瀀爀攀猀猀戀愀攀愀搀搀愀攀戀搀搀椀氀攀尀尀尀尀倀吀最琀愀猀猀渀樀攀挀琀椀漀渀愀琀攀瀀爀瀀洀匀攀焀椀渀攀匀愀洀瀀氀攀一愀洀攀倀漀挀愀琀椀漀渀倀挀焀伀瀀攀爀愀琀漀爀匀夀匀吀渀樀匀瀀攀挀刀攀瀀漀爀琀攀搀匀渀琀攀最爀愀琀椀漀渀渀樀嘀漀氀甀洀攀甀氀挀焀攀琀栀漀搀尀匀尀愀琀愀尀尀尀尀倀伀匀一渀愀氀礀猀椀猀攀琀栀漀搀尀匀尀愀琀愀尀尀尀尀倀伀匀一愀琀愀氀漀最一漀夀愀琀挀栀攀琀栀漀搀渀昀漀漀戀椀氀攀倀栀愀猀攀眀愀琀攀爀吀一吀爀愀搀椀攀渀琀琀漀眀椀琀栀椀渀洀椀渀氀漀眀刀愀琀攀洀氀洀椀渀漀氀甀洀渀匀甀渀椀爀攀洀洀甀洀刀倀伀瘀攀渀吀攀洀瀀攀爀愀琀甀爀攀洀椀渀洀

11、唀匀椀最刀攀昀漀昀昀洀椀渀洀唀匀椀最刀攀昀漀昀昀洀椀渀洀嘀匀匀匀椀最渀愀氀洀椀渀匀吀匀椀氀攀匀倀倀漀猀匀挀愀渀爀愀最洀椀渀漀渀匀吀愀爀最攀琀愀猀猀倀漀猀椀琀椀瘀攀渀琀攀最爀愀琀椀漀渀刀攀猀甀氀琀猀昀漀爀匀椀最刀攀昀漀昀昀刀攀琀吀椀洀圀椀搀琀栀爀攀愀攀椀最栀琀爀攀愀匀簀簀簀簀簀簀簀渀琀攀最爀愀琀椀漀渀刀攀猀甀氀琀猀昀漀爀匀椀最刀攀昀漀昀昀刀攀琀吀椀洀圀椀搀琀栀爀攀愀攀椀最栀琀爀攀愀匀簀簀簀簀簀簀簀匀刀攀瀀漀爀琀昀爀漀洀渀猀琀爀甀洀攀渀琀匀匀匀夀匀吀倀愀最攀漀昀渀琀攀最爀愀琀椀漀渀刀攀猀甀氀琀猀昀漀爀匀匀匀椀最渀愀氀刀攀琀吀椀洀圀椀搀琀栀爀攀愀攀椀最栀琀爀攀愀匀簀簀簀簀簀簀簀渀琀攀最爀愀琀椀漀渀刀

12、攀猀甀氀琀猀昀漀爀匀吀匀椀氀攀刀攀琀吀椀洀圀椀搀琀栀爀攀愀攀椀最栀琀爀攀愀匀簀簀簀簀簀簀簀匀刀攀瀀漀爀琀昀爀漀洀渀猀琀爀甀洀攀渀琀匀匀匀夀匀吀倀愀最攀漀昀刀攀琀吀椀洀攀最琀最琀最琀洀稀匀倀倀漀猀椀琀椀瘀攀匀刀攀瀀漀爀琀昀爀漀洀渀猀琀爀甀洀攀渀琀匀匀匀夀匀吀倀愀最攀漀昀渀搀漀昀刀攀瀀漀爀琀匀刀攀瀀漀爀琀昀爀漀洀渀猀琀爀甀洀攀渀琀匀匀匀夀匀吀倀愀最攀漀昀攀搀栀攀洀砀瀀爀攀猀猀靓(頀椁匀%谀椁簂椁頀椁讀缁缀徉砀螏頀h氀椀眂椃椌椌蔌餌攀氀漀琀攀挀愀渀栀礀搀爀漀挀栀氀漀爀椀搀攀伀攀搀栀攀洀砀瀀爀攀猀猀瀀搀昀瀀椀挀最椀昀攀氀漀琀攀挀愀渀栀礀搀爀漀挀栀氀漀爀椀搀攀伀攀搀栀攀洀砀瀀爀攀猀猀瀀搀昀尀尀昀戀愀愀愀

13、愀挀挀愀搀攀攀洀圀氀漀爀猀伀樀娀栀嘀欀瀀一攀爀伀眀匀唀爀瘀甀昀猀愀爀倀焀洀爀稀眀攀氀漀琀攀挀愀渀栀礀搀爀漀挀栀氀漀爀椀搀攀伀攀搀栀攀洀砀瀀爀攀猀猀愀昀愀愀攀挀昀攀昀愀戀愀渀栀椀戀椀琀漀爀猀最漀渀椀猀琀猀匀挀爀攀攀渀椀渀最椀戀爀愀爀椀攀猀眀眀眀攀搀栀攀洀砀瀀爀攀猀猀挀漀洀攀爀琀椀昀椀挀愀琀攀漀昀渀愀氀礀猀椀猀倀夀匀一倀刀伀倀刀吀匀漀氀攀挀甀氀愀爀漀爀洀甀氀愀氀一伀漀氀攀挀甀氀愀爀圀攀椀最栀琀匀琀漀爀愀最攀倀漀眀搀攀爀礀攀愀爀猀礀攀愀爀猀渀猀漀氀瘀攀渀琀洀漀渀琀栀猀洀漀渀琀栀栀攀洀椀挀愀氀匀琀爀甀挀琀甀爀攀一夀吀吀瀀瀀攀愀爀愀渀挀攀椀最栀琀礀攀氀氀漀眀琀漀礀攀氀氀漀眀匀漀氀椀搀一刀匀瀀攀挀琀爀甀洀

14、漀渀猀椀猀琀攀渀琀眀椀琀栀猀琀爀甀挀琀甀爀攀匀漀渀猀椀猀琀攀渀琀眀椀琀栀猀琀爀甀挀琀甀爀攀倀甀爀椀琀礀匀漀渀挀氀甀猀椀漀渀吀栀攀瀀爀漀搀甀挀琀栀愀猀戀攀攀渀琀攀猀琀攀搀愀渀搀挀漀洀瀀氀椀攀猀眀椀琀栀琀栀攀最椀瘀攀渀猀瀀攀挀椀昀椀挀愀琀椀漀渀猀倀爀漀搀甀挀琀一愀洀攀攀氀漀琀攀挀愀渀栀礀搀爀漀挀栀氀漀爀椀搀攀愀琀一漀夀匀一漀愀琀挀栀一漀栀攀洀椀挀愀氀一愀洀攀倀礀爀愀渀漀嬀崀椀渀搀漀氀椀稀椀渀漀嬀戀崀焀甀椀渀漀氀椀渀攀搀椀漀渀攀攀琀栀礀氀栀礀搀爀漀砀礀嬀嬀洀攀琀栀礀氀攀琀栀礀氀愀洀椀渀漀崀攀琀栀礀氀崀栀礀搀爀漀挀栀氀漀爀椀搀攀匀愀甀琀椀漀渀倀爀漀搀甀挀琀栀愀猀渀漀琀戀攀攀渀昀甀氀氀礀瘀愀氀椀搀愀琀攀搀昀漀爀洀攀搀椀挀愀氀愀瀀瀀氀椀挀愀琀椀漀渀猀漀爀爀攀猀攀愀爀挀栀甀猀攀漀渀氀礀吀攀氀愀砀洀愀椀氀琀攀挀栀攀搀栀攀洀砀瀀爀攀猀猀挀漀洀搀搀爀攀猀猀攀攀爀倀愀爀欀爀匀甀椀琀攀儀漀渀洀漀甀琀栀甀渀挀琀椀漀渀一唀匀眀眀眀攀搀栀攀洀砀瀀爀攀猀猀挀漀洀攀搀栀攀洀砀瀀爀攀猀猀靓言茀渀7椁脊