Amiodarone-hydrochloride-LCMS-12138-MedChemExpress.pdf

1、 File D:CHEM321DATACPKCPK2017-216-12138.D Tgt Mass (EZX): 681.80 Injection Date : 16-Feb-17, 12:03:44 Seq. Line : 0Sample Name : CPK2017-216-12138 Location : P1-B-06Acq. Operator : GZZ_718 Inj : 0Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:Chem321METHODS1-POS-3MIN.MAnalysis Meth

2、od : D:CHEM321METHODSSIM-HM-174C_005-H01GI03(0.0.05%TFA).MCatalog No : HY-14188 Batch#12138 Easy-Access Method: 1-POS-3MIN 681.80Method Info : Postive,MS:100-1000,Column ID:A-RP-85,50min0.5 1 1.5 2 2.5mAU0250500750DAD1 B, Sig=214,4 Ref=off 1.4191.4831.5151.5721.6061.644min0.5 1 1.5 2 2.5mAU0200400DA

3、D1 C, Sig=254,4 Ref=off 1.4721.5711.5931.644min0.5 1 1.5 2 2.50100000200000300000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.691min0.5 1 1.5 2 2.5050100150200Ion 682.8, MSD1 682.8,Target Mass 681.8 +H Positive, EIC=682.5:683.5 0.4761.8682.3212.5672.656Integration Results for DAD1 B, Sig=214,4 Ref

4、=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.42 0.02 1.60 1.13 0.08 1411.48 0.02 0.41 0.37 0.02 1411.52 0.02 0.40 0.06 0.02 1411.57 0.02 0.65 0.48 0.03 1411.61 0.01 1.41 2.30 0.07 1411.64 0.03 2016.34 1050.77 99.78 646Integration Results for DAD1 C, Sig=254,4 Ref=offRetTim Width Area Heigh

5、t Area% MS(+)|-|-|-|-|-|-|1.47 0.02 0.40 0.04 0.03 1411.57 0.04 0.51 0.23 0.04 1411.59 0.01 1.18 0.12 0.10 1411.64 0.03 1161.30 605.44 99.82 646MS Report from Instrument: HY-LCMS-02HY-LCMS-02 2/16/2017 1:16:45 PM GZZ_718 Page 1 of 2Ret. Time: 1.69 m/z200 300 400 500 600 700 800 90001000020000300004000050000600007000080000ES-API Positive647.0646.0MS Report from Instrument: HY-LCMS-02HY-LCMS-02 2/16/2017 1:16:45 PM GZZ_718 Page 2 of 2