1、 File .0182018041720180417-1CPK2018-416-15607.D Tgt Mass (CHM):Injection Date : 17 Apr 18 6:46 pm +0800 Seq. Line : 74Sample Name : CPK2018-416-15607 Location : P1-F-08Acq. Operator : SYSTEM Inj : 1Spec. Reported : MS Integration Inj Volume : 2 ulAcq. Method : D:LCMS03Data20182018041720180417-11-POS
2、-3MIN.MAnalysis Method : D:LCMS03Data20182018041720180417-11-POS-3MIN.MCatalog No : HY-12764 Batch#15607Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temperature : 45Cmin0 0.5 1 1.
3、5 2 2.5mAU0200DAD1 A, Sig=214,4 Ref=off1.3521.4711.4921.6451.7481.9992.0962.1492.3082.345min0 0.5 1 1.5 2 2.5mAU0500DAD1 B, Sig=254,4 Ref=off1.4841.4971.5601.6451.7222.0232.0972.1372.1572.296min0 0.5 1 1.5 2 2.5mV0100ELS1 A, ELSD Signal1.717min0 0.5 1 1.5 2 2.501000000MSD1 TIC, MS File ES-API, Pos,
4、Scan, Frag: 701.673min0 0.5 1 1.5 2 2.50250000500000750000Ion 240.3, MSD1 240.3,Target Mass 239.3 +H Positive, EIC=240:2411.671Integration Results for DAD1 A, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.35 0.03 2.14 1.07 0.37 1301.47 0.01 0.40 0.61 0.07 2331.49 0.02 1.31 1.19
5、 0.23 1021.64 0.02 562.26 494.13 97.53 2401.75 0.01 0.55 0.03 0.10 2332.00 0.03 2.42 0.93 0.42 4382.10 0.01 0.49 0.59 0.09 1052.15 0.02 3.74 2.32 0.65 1052.31 0.09 1.57 0.30 0.27 1052.34 0.02 1.65 1.13 0.29 105Integration Results for DAD1 B, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|
6、-|-|-|-|1.48 0.02 0.33 0.33 0.03 2331.50 0.02 1.30 1.14 0.10 1021.56 0.02 0.24 0.18 0.02 2331.64 0.02 1271.63 1115.90 99.61 240MS Report from Instrument: LCMS-03LCMS-03 4/18/2018 9:57:28 AM SYSTEM Page 1 of 41.72 0.01 0.88 1.14 0.07 2402.02 0.02 0.70 0.69 0.05 4382.10 0.01 0.23 0.30 0.02 1052.14 0.0
7、1 0.37 0.42 0.03 1052.16 0.01 0.13 0.16 0.01 1052.30 0.03 0.85 0.40 0.07 105Integration Results for ELS1 A, ELSD SignalRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.72 0.05 614.42 192.67 100.00 240Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.67 0.0
8、6 7094469.00 1959734.38 100.00 240MS Report from Instrument: LCMS-03LCMS-03 4/18/2018 9:57:28 AM SYSTEM Page 2 of 4Ret. Time: 1.67 m/z100 200 300 400 500 600 700 800 900020000400006000080000100000120000140000160000180000ES-API Positive233.1502.3480.3479.4240.1MS Report from Instrument: LCMS-03LCMS-0
9、3 4/18/2018 9:57:28 AM SYSTEM Page 3 of 4* End of Report *MS Report from Instrument: LCMS-03LCMS-03 4/18/2018 9:57:28 AM SYSTEM Page 4 of 4 Inhibitors, Agonists, Screening Librarieswww.MedChemESafety Data SheetRevision Date:Oct.-09-2018Print Date: Oct.-09-20181. PRODUCT AND COMPANY IDENTIFICATION1.1
10、 Product identifierProduct name : A-836339Catalog No. : HY-12761CAS No. : 959746-77-11.2 Relevant identified uses of the substance or mixture and uses advised againstIdentified uses : Laboratory chemicals, manufacture of substances.1.3 Details of the supplier of the safety data sheetCompany: MedChem
11、Express USATel: 609-228-6898Fax: 609-228-5909E-mail: 1.4 Emergency telephone numberEmergency Phone #: 609-228-68982. HAZARDS IDENTIFICATION2.1 Classification of the substance or mixtureNot a hazardous substance or mixture.2.2 GHS Label elements, including precautionary statementsNot a hazardous subs
12、tance or mixture.2.3 Other hazardsNone.3. COMPOSITION/INFORMATION ON INGREDIENTS3.1 SubstancesSynonyms: NoneFormula: C16H26N2O2SMolecular Weight: 310.45CAS No. : 959746-77-14. FIRST AID MEASURES4.1 Description of first aid measuresEye contactRemove any contact lenses, locate eye-wash station, and fl
13、ush eyes immediately with large amounts of water. Separate eyelidswith fingers to ensure adequate flushing. Promptly call a physician.Skin contactRinse skin thoroughly with large amounts of water. Remove contaminated clothing and shoes and call a physician.Page 1 of 5 www.MedChemEInhalationImmediate
14、ly relocate self or casualty to fresh air. If breathing is difficult, give cardiopulmonary resuscitation (CPR). Avoid mouth-to-mouth resuscitation.IngestionWash out mouth with water; Do NOT induce vomiting; call a physician.4.2 Most important symptoms and effects, both acute and delayedThe most impo
15、rtant known symptoms and effects are described in the labelling (see section 2.2).4.3 Indication of any immediate medical attention and special treatment neededTreat symptomatically.5. FIRE FIGHTING MEASURES5.1 Extinguishing mediaSuitable extinguishing mediaUse water spray, dry chemical, foam, and c
16、arbon dioxide fire extinguisher.5.2 Special hazards arising from the substance or mixtureDuring combustion, may emit irritant fumes.5.3 Advice for firefightersWear self-contained breathing apparatus and protective clothing.6. ACCIDENTAL RELEASE MEASURES6.1 Personal precautions, protective equipment
17、and emergency proceduresUse full personal protective equipment. Avoid breathing vapors, mist, dust or gas. Ensure adequate ventilation. Evacuate personnelto safe areas.Refer to protective measures listed in sections 8.6.2 Environmental precautionsTry to prevent further leakage or spillage. Keep the
18、product away from drains or water courses.6.3 Methods and materials for containment and cleaning upAbsorb solutions with finely-powdered liquid-binding material (diatomite, universal binders); Decontaminate surfaces andequipment by scrubbing with alcohol; Dispose of contaminated material according t
19、o Section 13.7. HANDLING AND STORAGE7.1 Precautions for safe handlingAvoid inhalation, contact with eyes and skin. Avoid dust and aerosol formation. Use only in areas with appropriate exhaustventilation.7.2 Conditions for safe storage, including any incompatibilitiesKeep container tightly sealed in
20、cool, well-ventilated area. Keep away from direct sunlight and sources of ignition.Recommended storage temperature:Powder-20C 3 years4C 2 yearsIn solvent-80C 6 months-20C 1 monthShipping at room temperature if less than 2 weeks.7.3 Specific end use(s)No data available.8. EXPOSURE CONTROLS/PERSONAL P
21、ROTECTION8.1 Control parametersPage 2 of 5 www.MedChemEComponents with workplace control parametersThis product contains no substances with occupational exposure limit values.8.2 Exposure controlsEngineering controlsEnsure adequate ventilation. Provide accessible safety shower and eye wash station.P
22、ersonal protective equipmentEye protection Safety goggles with side-shields.Hand protection Protective gloves.Skin and body protection Impervious clothing.Respiratory protection Suitable respirator.Environmental exposure controlsKeep the product away from drains, water courses or the soil. Cleanspil
23、lages in a safe way as soon as possible.9. PHYSICAL AND CHEMICAL PROPERTIES9.1 Information on basic physical and chemical propertiesAppearance Light yellow to yellow (Solid)Odor No data availableOdor threshold No data availablepH No data availableMelting/freezing point No data availableBoiling point
24、/range No data availableFlash point No data availableEvaporation rate No data availableFlammability (solid, gas) No data availableUpper/lower flammability or explosive limitsNo data availableVapor pressure No data availableVapor density No data availableRelative density No data availableWater Solubi
25、lity No data availablePartition coefficient No data availableAuto-ignition temperature No data availableDecomposition temperature No data availableViscosity No data availableExplosive properties No data availableOxidizing properties No data available9.2 Other safety informationNo data available.10.
26、STABILITY AND REACTIVITY10.1 ReactivityNo data available.10.2 Chemical stabilityStable under recommended storage conditions.10.3 Possibility of hazardous reactionsPage 3 of 5 www.MedChemENo data available.10.4 Conditions to avoidNo data available.10.5 Incompatible materialsStrong acids/alkalis, stro
27、ng oxidising/reducing agents.10.6 Hazardous decomposition productsUnder fire conditions, may decompose and emit toxic fumes.Other decomposition products - no data available.11.TOXICOLOGICAL INFORMATION11.1 Information on toxicological effectsAcute toxicityClassified based on available data. For more
28、 details, see section 2Skin corrosion/irritationClassified based on available data. For more details, see section 2Serious eye damage/irritationClassified based on available data. For more details, see section 2Respiratory or skin sensitizationClassified based on available data. For more details, se
29、e section 2Germ cell mutagenicityClassified based on available data. For more details, see section 2CarcinogenicityIARC: No component of this product present at a level equal to or greater than 0.1% is identified as probable, possible orconfirmed human carcinogen by IARC.ACGIH: No component of this
30、product present at a level equal to or greater than 0.1% is identified as a potential or confirmedcarcinogen by ACGIH.NTP: No component of this product present at a level equal to or greater than 0.1% is identified as a anticipated or confirmedcarcinogen by NTP.OSHA: No component of this product pre
31、sent at a level equal to or greater than 0.1% is identified as a potential or confirmedcarcinogen by OSHA.Reproductive toxicityClassified based on available data. For more details, see section 2Specific target organ toxicity - single exposureClassified based on available data. For more details, see section 2Specifi
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