5-6-Carboxyfluorescein-LCMS-15337-MedChemExpress.pdf

1、 File .Data2017121720171217CPK2017-D13-15337.D Tgt Mass (CHM):Injection Date : 17 Dec 17 12:15 pm +0800 Seq. Line : 26Sample Name : CPK2017-D13-15337 Location : P2-E-02Acq. Operator : ZLJ_587 Inj : 1Spec. Reported : MS Integration Inj Volume : 1 ulAcq. Method : D:LCMS03Data20171217201712171-POS-3MIN

2、.MAnalysis Method : D:LCMS03Data20171217201712171-POS-3MIN.MCatalog No : HY-15940 Batch#15337Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temperature : 45Cmin0 0.5 1 1.5 2 2.5mAU0

3、5001000DAD1 A, Sig=214,4 Ref=off1.2271.3071.3891.4301.4601.4941.5351.6081.670min0 0.5 1 1.5 2 2.5mAU0100200DAD1 B, Sig=254,4 Ref=off1.2281.2701.3891.4411.4951.5331.6051.6792.026min0 0.5 1 1.5 2 2.5mV50100ELS1 A, ELSD Signal1.562min0 0.5 1 1.5 2 2.5200000400000600000MSD1 TIC, MS File ES-API, Pos, Sca

4、n, Frag: 701.522min0 0.5 1 1.5 2 2.50200400Ion 753.7, MSD1 753.7,Target Mass 752.7 +H Positive, EIC=753.4:754.4Integration Results for DAD1 A, Sig=214,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.23 0.02 1.29 1.37 0.06 1571.31 0.02 16.98 17.46 0.85 1571.39 0.02 3.94 4.24 0.20 7021.43

5、0.01 1.23 0.09 0.06 2331.46 0.01 0.22 0.42 0.01 3771.49 0.02 1956.46 1677.37 97.36 3771.54 0.01 10.24 15.58 0.51 3771.61 0.03 14.87 8.92 0.74 3771.67 0.03 4.33 2.63 0.22 233Integration Results for DAD1 B, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.23 0.02 0.39 0.39 0.10 1571

6、.27 0.02 0.11 0.12 0.03 1571.39 0.02 1.52 1.40 0.38 7021.44 0.02 0.47 0.50 0.12 2331.50 0.02 385.89 330.48 97.32 377MS Report from Instrument: LCMS-03LCMS-03 12/18/2017 1:16:39 PM ZLJ_587 Page 1 of 41.53 0.01 3.55 4.39 0.90 3771.61 0.02 3.47 2.21 0.88 2331.68 0.03 0.83 0.50 0.21 2332.03 0.02 0.26 0.

7、28 0.07 105Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.52 0.06 2620782.00 714633.50 100.00 377MS Report from Instrument: LCMS-03LCMS-03 12/18/2017 1:16:39 PM ZLJ_587 Page 2 of 4Ret. Time: 1.52 m/z100 200 300 400 500 600 700 800 900020000400006000080000100000ES-API Positive105.1233.2378.1377.1MS Report from Instrument: LCMS-03LCMS-03 12/18/2017 1:16:39 PM ZLJ_587 Page 3 of 4* End of Report *MS Report from Instrument: LCMS-03LCMS-03 12/18/2017 1:16:39 PM ZLJ_587 Page 4 of 4