5-6-FAM-SE-LCMS-15324-MedChemExpress.pdf

1、 File .20182018022720180227CPK2018-223-15324.D Tgt Mass (CHM):Injection Date : 27 Feb 18 2:05 pm +0800 Seq. Line : 64Sample Name : CPK2018-223-15324 Location : P1-D-10Acq. Operator : SYSTEM Inj : 1Spec. Reported : MS Integration Inj Volume : 2 ulAcq. Method : D:LCMS03Data201820180227201802271-POS-3M

2、IN.MAnalysis Method : D:LCMS03Data201820180227201802271-POS-3MIN.MCatalog No : HY-15937 Batch#15324Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA)Gradient: 5% to 95%B within 1.3 minFlow Rate :1.8ml/minColumn :SunFire C18, 4.6*50mm,3.5um A-RP-186Oven Temperature : 45Cmin0 0.5 1 1.5 2 2

3、.5mAU0100200300400DAD1 B, Sig=254,4 Ref=off1.4571.5011.5811.7632.026min0 0.5 1 1.5 2 2.5mV50100ELS1 A, ELSD Signal1.649min0 0.5 1 1.5 2 2.5200000400000600000MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.609min0 0.5 1 1.5 2 2.50100200300400Ion 947.8, MSD1 947.8,Target Mass 946.8 +H Positive, EIC=947

4、.5:948.5Integration Results for DAD1 B, Sig=254,4 Ref=offRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.46 0.02 3.32 3.13 0.63 2331.50 0.02 5.63 5.50 1.07 2331.58 0.02 514.48 491.53 98.04 4741.76 0.01 0.38 0.45 0.07 2332.03 0.01 0.94 1.14 0.18 233Integration Results for ELS1 A, ELSD SignalRetTim

5、 Width Area Height Area% MS(+)|-|-|-|-|-|-|1.65 0.05 456.30 149.78 100.00 474Integration Results for MSD1 TIC, MS FileRetTim Width Area Height Area% MS(+)|-|-|-|-|-|-|1.61 0.06 2111790.00 566876.94 100.00 474MS Report from Instrument: LCMS-03LCMS-03 3/1/2018 11:18:10 AM SYSTEM Page 1 of 3Ret. Time: 1.61 m/z100 200 300 400 500 600 700 800 900020000400006000080000100000ES-API Positive476.1105.1 233.1475.1474.1MS Report from Instrument: LCMS-03LCMS-03 3/1/2018 11:18:10 AM SYSTEM Page 2 of 3* End of Report *MS Report from Instrument: LCMS-03LCMS-03 3/1/2018 11:18:10 AM SYSTEM Page 3 of 3